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Thin-layer and gas chromatography: OCR A‑Level Chemistry A questions

OCR A-Level Chemistry A past-paper questions on 6.3.1.1 Thin-layer and gas chromatography, 2016–2025, with mark schemes and examiner’s reports where available.

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  1. Q22(a)(i)

    June 2025 · Paper 2

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  2. Q13

    June 2024 · Paper 2

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  3. Q5(a)(i)

    June 2024 · Paper 3

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  5. Q10

    November 2021 · Paper 2

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  6. Q13

    November 2020 · Paper 2

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  7. Q17(b)(i)

    June 2019 · Paper 2

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  8. Q17(b)(ii)

    June 2019 · Paper 2

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  9. Q21(c)(i)

    June 2018 · Paper 2

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All 9 questions on Thin-layer and gas chromatography, as a list
  1. June 2025, Paper 2, Q22(a)(i) (1 mark): Determine the Rf values of the two α-amino acids in the chromatogram. [1]
  2. June 2024, Paper 2, Q13 (1 mark): A sample containing a mixture of 3 components, X, Y and Z, is analysed using gas chromatography. The gas chromatogram below is obtained. The relative peak areas
  3. June 2024, Paper 3, Q5(a)(i) (1 mark): Determine the Rf value of propan-1-ol. Show your working. Rf = [1]
  4. June 2024, Paper 3, Q5(a)(iii) (3 marks): A student investigates the alkaline hydrolysis of 1-chloropropane using the same method as for 1-bromopropane. Predict, with reasons, how the appearance of the
  5. November 2021, Paper 2, Q10 (1 mark): A TLC chromatogram for two compounds is shown below. solvent front origin What is the Rf value for the compound that is most strongly adsorbed onto the stationa
  6. November 2020, Paper 2, Q13 (1 mark): Which statement(s) is/are correct for gas chromatography? 1 The components in a mixture can be identified from their retention time. 2 The relative peak areas g
  7. June 2019, Paper 2, Q17(b)(i) (1 mark): What is the Rf value of serine (ser) in solvent W? Rf = [1]
  8. June 2019, Paper 2, Q17(b)(ii) (2 marks): Analyse the chromatograms to identify the unknown amino acid. Explain your reasoning. Name of unknown amino acid Explanation [2]
  9. June 2018, Paper 2, Q21(c)(i) (2 marks): The concentration of ester K in the cosmetic product is 9.13 × 10−2 g dm−3. Using the results, calculate the concentration, in mol dm−3, of ester M in the cosme

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